Project N° Unit Doc. Type Mat. Code Serial N° Rev.

Page

068107C001 000 JSS 1300 016 A 1/6

PROJECT : BS-IV PROJECT.

The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,

LOCATION : IOCL, BARAUNI REFINERY.

disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

OWNER EPCM

TECHNIP INDIA LTD.

INDIAN OIL CORPORATION LIMITED. NOIDA, INDIA.

SPECIAL REQUIREMENTS

FOR

HYDROGEN SERVICE (H2)

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(Use “X” Mark)
Approval Review

Information

Pages modified under this revision: none.

A 18-12-2015 ISSUE FOR REVIEW SVRH SRR MAH

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DOCUMENT REVISIONS
This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization
Project N° Unit Document Code Serial N° Rev. Page

068107C001 000 JSS 1300 016 A 2/6

TECHNIP INDIA LTD.

SPECIAL REQUIREMENTSFOR HYDROGEN SERVICE (H2)

CONTENTS

Description Page No.

The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,
disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

CONTENTS 2

1.0 GENERAL 3

2.0 PIPE, FLANGES & FITTINGS 3

3.0 VALVES 4

This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization
Project N° Unit Document Code Serial N° Rev. Page

068107C001 000 JSS 1300 016 A 3/6

TECHNIP INDIA LTD.

SPECIAL REQUIREMENTSFOR HYDROGEN SERVICE (H2)

1.0 GENERAL
The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,

These requirements are applicable in addition to the requirements specified in the Piping
Material Specifications.
disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

2.0 PIPES, FLANGES AND FITTINGS

2.1 Method of Manufacture

2.1.1 All carbon steel pipes, fittings and flanges having wall thickness 9.53 mm and above
shall be normalized. Cold drawn pipes and fittings shall be normalized after the final
cold draw pass for all thicknesses. In addition, fittings made from forgings shall have
Carbon - 0.35% max. and Silicon - 0.35% max. The normalizing heat treatment shall be
a separate heating operation and not a part of the hot forming operation

2.1.2 All alloy steel (Cr-Mo) pipes, forgings and fittings shall be normalized and tempered.
The normalizing and tempering shall be a separate heating operation and not a part of
the hot forming operation. The maximum room temperature tensile strength shall be
100,000 psi.
2.1.3 For 9Cr-1Mo-V Grade 91 material all requirement s shall be as per API 938 B-2008.
For Pipes, fittings, flanges, valves and other piping components.

2.2 Post Weld Heat Treatment

2.2.1 All carbon steel pipes and fittings having wall thickness 19 mm and above shall be post
weld heat treated.

2.2.2 All alloy steel (Cr-Mo) pipes and fittings shall be post weld heat treated irrespective of
type or thickness of weld.

2.2.3 All austenitic stainless steel grades shall be solution annealed after welding. 100%
radiography of welded joints shall be done both before and after PWHT.

2.3 Ferrite No. Test

2.3.1 For all austenitic stainless steels, the weld deposit shall be checked for ferrite content. A
Ferrite No. (FN) not less than 3% and not more than 10% is required to avoid sigma
phase embitterment during heat treatment. FN shall be determined by Ferritescope or
may be calculated by using the schaffler or DeLong diagrams (DeLong diagram should
be used if FCAW is performed), prior to post weld heat treatment.

This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization
Project N° Unit Document Code Serial N° Rev. Page

068107C001 000 JSS 1300 016 A 4/6

TECHNIP INDIA LTD.

SPECIAL REQUIREMENTSFOR HYDROGEN SERVICE (H2)

2.4 Impact Test

wall
2.4.1 For all carbon steels and alloy steels pipes, flanges and fittings with thickness over 19
The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,

mm, Charpy-V Notch impact testing shall be carried out in accordance with paragraph
UG-84 of ASME Section VIII, Div-1 for weld metal and base metal from the thickest item
disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

per heat of material and per heat treating batch. Impact test specimen shall be in
complete heat treated condition and in accordance with ASTM A370 Impact energies at
0 C shall average greater than 27J (20 ft-lb) per set of 3 specimens, with a minimum of
19J (15 ft-lb).

2.4.2 If welding is used in manufacture, impact test of Heat Affected Zone (HAZ) and weld
metal shall also be carried out.

2.5 Hardness

2.5.1 For carbon steel pipes and fittings, hardness of weld and HAZ shall be limited to 200
BHN (max.).

2.5.2 For alloy steel pipes and fittings, hardness of weld and HAZ shall be limited to 225 BHN
(max.).

2.6 Radiography

2.6.1 All girth welded joints (longitudinal and circumferential) shall be 100% radiographed in
accordance with UW-51 of ASME Section VIII, Div-1 and ASME Section V. Radiography
shall be performed after post weld heat treatment.

3.0 VALVES

3.1 All valve castings shall be of radiographic quality. The requirement of radiography shall be
as per Technical Notes for Valves and Valve Material Specifications.

3.2 All cast valve flanges & bodies with flange rating of Class 900 or greater shall be
examined in accordance with paragraphs 7.2 through 7.5 of Appendix-7 of ASME SEC-
VIII, DIV.1, regardless of casting quality factor.

3.3 Only Normalized and Tempered material shall be used in the following specifications:
Castings: A217Gr.WC1, A217Gr.WC4, A21Gr.WC5,
A217Gr.WC6, A217 Gr.WC9, A217 Gr.C5, A217 Gr.C12
Forgings: A182 Gr.F11 Cl.2, A182 Gr.F22 Cl.3, A182 Gr.F5, A182 Gr.F9

This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization
Project N° Unit Document Code Serial N° Rev. Page

068107C001 000 JSS 1300 016 A 5/6

TECHNIP INDIA LTD.

SPECIAL REQUIREMENTSFOR HYDROGEN SERVICE (H2)

3.4 Body / bonnet / cover joints & stuffing box of all valves shall have low emission and shall be
helium leak tested as per ASME Sec.V, Subsection A, Article 10 (Detector Probe
The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,

Technique), Appendix IV at a minimum of 25% of the allowable (rated) cold working

pressure. Sampling for helium leak test shall be one valve selected at random per item
disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

no. of the requisition. The failure of helium leak test shall call for testing of remaining
valves of that item at vendor’s cost. Test duration shall be as follows:

Test Duration in Minutes

Nominal Pressure Class
Size
UPTO 300 600 800 & 900 1500 2500
Upto 2" 3 6 9 12 12
3" to 6" 6 9 12 15 18
8" to 16" 9 9 12 15 18
18" to 24" 9 12 15 18 21
The valve shall show no leakage. No leakage is defined as a total leakage rate of less than0.0001
ml/s of helium.

3.5 CS & AS Valves:

3.5.1 Bend test and Magnetic Particle inspection of the entire surface of body and
bonnet casting shall be in accordance with ASTM A217. Supplementary
requirement S3 & S4 evaluation of magnetic particle, inspection shall be in
accordance with MSS-SP-53 except that no linear discontinuities shall be
allowed.

3.5.2 The Brinell hardness of heat treated casting shall not exceed 200 BHN for carbon
steel & 225 for alloy steel.

3.5.3 Repair of defective casting shall be outlined in writing to the purchaser before
repair starts. Repair method to be approved prior to welding.

3.5.4 Casting shall be preheated to a minimum of 400 º F prior to welding and all Chromium-
Molybdenum alloys shall be post weld heat treated after welding is complete. Stress
relieving is essential for welds.

3.5.5 Carbon steel shall be normalized and alloy steels shall be normalized & tempered.

3.5.6 Dye Penetrant test of welds shall be in accordance with ASTM B165 Procedure B-2.
Interpretation as per Appendix-8 of ASME-VIII Div.1.

This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization
Project N° Unit Document Code Serial N° Rev. Page

068107C001 000 JSS 1300 016 A 6/6

TECHNIP INDIA LTD.

SPECIAL REQUIREMENTSFOR HYDROGEN SERVICE (H2)

3.5.7 The tensile stress for AS shall be less than 100,000 psi.

3.5.8 Charpy V-notch impact testing is to be done for valve material (average 20 ft-lb for set of
The present document or drawing is property of TECHNIP KT INDIA LTD. and shall not, under any circumstances, be totally or partially, directly or indirectly, transferred, reproduced, copied,

3 [minimum value 15 ft-lb] at 30ºF).

disclosed or used, without its prior written consent, for any purpose and in any way other than that for which it is specifically furnished or outside the extent of the agreed upon right of use.

3.5.9 For radiography and acceptance criteria for valve castings, refer Cl. 3.6.2

3.6 SS Valves:

3.6.1 Casting and test bar shall be heat treated together. Valve casting shall be in solution
heat treated and pickled condition.

3.6.2 Critical body and bonnet casing section typically defined by ASME B16.34 shall be
radiographed and shall meet ASTM E446 (upto 2" thick) Category A,B & CA Level 2,
Category CB, OC & CD Level 3, Category D,B & F Level 0. For wall thickness 2" to 4.5"
comparable plates of ASTM E186 shall be used. ASTM E94 and ASTM E142 shall be
used for recommended practice & controlling quality of radiography as guide. The entire
surface of all castings shall be dye-penetrant inspected after pickling.

3.6.3 Repair welds shall be 100% radiographed and evaluated in accordance with paragraph
344.5 of ASME B31.3 with a minimum casting quality factor of 0.95. Dye Penetration
test shall be as per ASTM E165 Procedure B-2, Interpretation as per Appendix-8 of
ASME-VIII Div.1.

This document developed by TECHNIP India Limited and the information it contains are property of Indian Oil Corporation
Ltd. It shall not be used for any purpose other than for which it was supplied.
CONFIDENTIAL – Not to disclose without Authorization